Inorganic Solid Phases

[Al₁₃(OH)₂₄(H₂O)₂₄]Cl₁₅·13H₂O (Al₁₃Cl₁₅[OH]₂₄[H₂O]₃₇) Crystal Structure

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General Information

Phase Label(s): Al₁₃Cl₁₅[OH]₂₄[H₂O]₃₇
Structure Class(es): –
Classification by Properties: –
Mineral Name(s): –
Pearson Symbol: mP360
Space Group: 14
Phase Prototype: Al₁₃Cl₁₅[OH]₂₄[H₂O]₃₇
Measurement Detail(s): automatic diffractometer; 25 (determination of cell parameters), automatic diffractometer; Enraf-Nonius CAD4 (determination of structural parameters), X-rays, Cu Kα; λ = 0.15418 nm (determination of cell and structural parameters), T = 293(2) K (determination of cell and structural parameters)
Phase Class(es): –
Compound Class(es): hydroxide, chloride, hydrate
Interpretation Detail(s): positions of non-H and part of H atoms determined, full-matrix least-squares refinement on F²; 903 variables; 11292 reflections; I > 2σ(I), R = 0.0527; wR = 0.1341
Sample Detail(s): sample prepared from AlCl₃[H₂O]₆, single crystal (determination of cell parameters), single crystal, 0.15×0.20×0.20 mm³ (determination of structural parameters)

Substance Summary

Standard Formula: Al₁₃Cl₁₅[OH]₂₄[H₂O]₃₇
Alphabetic Formula: Al₁₃Cl₁₅[H₂O]₃₇[OH]₂₄
Published Formula: [Al₁₃(OH)₂₄(H₂O)₂₄]Cl₁₅·13H₂O
Refined Formula: Al₁₃Cl_14.99H₇₈O₆₁
Wyckoff Sequence: 14,e⁸⁹da
Z Formula Units: 4
Density: ρ = 1.78 Mg·m⁻³

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Crystallographic Data

Cell Parameters

	Published Data	Standardized Data
	Published Data	Unit Cell	Niggli-Reduced Cell
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a
b
c
α
β
γ
a/b
b/c
c/a
V

Atom Coordinates

Standardized

Site	Element	Wyckoff Symbol	Symmetry	X	Y	Z	Occupation	Co-ord. No.	Atomic Env.
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Published

Site	Element	Wyckoff Symbol	Symmetry	X	Y	Z	Occupation
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Displacement Parameters

Isotropic

Site	Published U [nm²]	Type	Computed B_eq [nm²]
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Anisotropic

Site	U₁₁ [nm²]	U₂₂ [nm²]	U₃₃ [nm²]	U₁₂ [nm²]	U₁₃ [nm²]	U₂₃ [nm²]
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Experimental Details

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Reference

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3D Interactive Structure

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About this content

Database name

PAULING FILE Multinaries Edition – 2012

Dataset ID

sd_1601466

Copyright

©Springer & Material Phases Data System (MPDS), Switzerland & National Institute for Materials Science (NIMS), Japan, 2016

Chief Editor

Pierre Villars, Material Phases Data System (MPDS), CH-6354 Vitznau, Switzerland

villars.mpds@bluewin.ch

Credits

SpringerMaterials Release 2016.

Project Coordinator: Shuichi Iwata

Section-Editor: Karin Cenzual (Crystal Structures)

Cite this content

Pierre Villars (Chief Editor), PAULING FILE in: Inorganic Solid Phases, SpringerMaterials (online database), Springer, Heidelberg (ed.) SpringerMaterials [Al13(OH)24(H2O)24]Cl15·13H2O (Al13Cl15[OH]24[H2O]37) Crystal Structure sd_1601466 (Springer-Verlag GmbH, Heidelberg, © 2016)

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