Inorganic Solid Phases

K₁₅[Dy₂(H₂O)₂(SbW₉O₃₃)(W₅O₁₈)₂]·22H₂O (K₁₅Dy₂W₁₉SbO₆₉[H₂O]₂₄) Crystal Structure

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General Information

Phase Label(s): K₁₅Dy₂W₁₉SbO₆₉[H₂O]₂₄
Structure Class(es): –
Classification by Properties: –
Mineral Name(s): –
Pearson Symbol: aP266
Space Group: 2
Phase Prototype: K₁₅Dy₂W₁₉SbO₆₉[H₂O]₂₄
Measurement Detail(s): automatic diffractometer (determination of cell parameters), automatic diffractometer; Rigaku R-AXIS RAPID (determination of structural parameters), X-rays, Mo Kα; λ = 0.071069 nm (determination of cell and structural parameters)
Phase Class(es): –
Compound Class(es): oxide, hydrate
Interpretation Detail(s): positions of non-H atoms determined, full-matrix least-squares refinement; 1088 variables; 28123 reflections; I > 2σ(I), R = 0.076; wR = 0.167
Sample Detail(s): sample prepared from Sb₂O₃ (valentinite), tungstate solution, Dy₂O₃, X-ray fluorescence spectroscopy; 57 wt.% W, 10 wt.% K, 6.3 wt.% Dy, 1.8 wt.% Sb, single crystal (determination of cell and structural parameters)

Substance Summary

Standard Formula: K₁₅Dy₂W₁₉SbO₆₉[H₂O]₂₄
Alphabetic Formula: Dy₂[H₂O]₂₄K₁₅O₆₉SbW₁₉
Published Formula: K₁₅[Dy₂(H₂O)₂(SbW₉O₃₃)(W₅O₁₈)₂]·22H₂O
Refined Formula: Dy₂H₄₈K₁₅O₉₃SbW₁₉
Wyckoff Sequence: 2,i¹³³
Z Formula Units: 2
Density: ρ = 4.09 Mg·m⁻³

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Crystallographic Data

Cell Parameters

	Published Data	Standardized Data
	Published Data	Unit Cell	Niggli-Reduced Cell
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a
b
c
α
β
γ
a/b
b/c
c/a
V

Atom Coordinates

Standardized

Site	Element	Wyckoff Symbol	Symmetry	X	Y	Z	Occupation	Co-ord. No.	Atomic Env.
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Published

Site	Element	Wyckoff Symbol	Symmetry	X	Y	Z	Occupation
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Displacement Parameters

Isotropic

Site	Published U [nm²]	Type	Computed B_eq [nm²]
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Anisotropic

Site	U₁₁ [nm²]	U₂₂ [nm²]	U₃₃ [nm²]	U₁₂ [nm²]	U₁₃ [nm²]	U₂₃ [nm²]
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Experimental Details

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Reference

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3D Interactive Structure

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About this content

Database name

PAULING FILE Multinaries Edition – 2012

Dataset ID

sd_1827636

Copyright

©Springer & Material Phases Data System (MPDS), Switzerland & National Institute for Materials Science (NIMS), Japan, 2016

Chief Editor

Pierre Villars, Material Phases Data System (MPDS), CH-6354 Vitznau, Switzerland

villars.mpds@bluewin.ch

Credits

SpringerMaterials Release 2016.

Project Coordinator: Shuichi Iwata

Section-Editor: Karin Cenzual (Crystal Structures)

Cite this content

Pierre Villars (Chief Editor), PAULING FILE in: Inorganic Solid Phases, SpringerMaterials (online database), Springer, Heidelberg (ed.) SpringerMaterials K15[Dy2(H2O)2(SbW9O33)(W5O18)2]·22H2O (K15Dy2W19SbO69[H2O]24) Crystal Structure sd_1827636 (Springer-Verlag GmbH, Heidelberg, © 2016)

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