Inorganic Solid Phases

K10H3[Dy(SiMo11O39)2]·29H2O (H3K10DyMo22[SiO4]2O70[H2O]29, T = 183 K) Crystal Structure

General Information

  • Phase Label(s): H3K10DyMo22[SiO4]2O70[H2O]29
  • Structure Class(es):
  • Classification by Properties:
  • Mineral Name(s):
  • Pearson Symbol: mP566
  • Space Group: 14
  • Phase Prototype: H3K10DyMo22[SiO4]2O70[H2O]29
  • Measurement Detail(s): automatic diffractometer (determination of cell parameters), automatic diffractometer; Nicolet R3m/E (determination of structural parameters), X-rays, Mo Kα (determination of cell and structural parameters), T = 183 K (determination of cell and structural parameters)
  • Phase Class(es):
  • Compound Class(es): orthosilicate, oxide, hydrate
  • Interpretation Detail(s): positions of non-H atoms determined, block-diagonal least-squares refinement; 7337 reflections; I > 3σ(I), R = 0.062; wR = 0.072
  • Sample Detail(s): sample prepared from Na2MoO4[H2O]2, HCl, Na2SiO3[H2O]9, Dy[NO3]3, glacial acetic acid, CH3COOK, chemical analysis; 8.82 wt.% K, 3.57 wt.% Dy, 1.32 wt.% Si, 46.96 wt.% Mo, 11.86 wt.% H2O, single crystal (determination of cell and structural parameters)

Substance Summary

  • Standard Formula: H3K10DyMo22[SiO4]2O70[H2O]29
  • Alphabetic Formula: DyH3[H2O]29K10Mo22O70[SiO4]2
  • Published Formula: K10H3[Dy(SiMo11O39)2]·29H2O
  • Refined Formula: DyH59K10Mo22O106.50Si2
  • Wyckoff Sequence: 14,e141a
  • Z Formula Units: 4
  • Density: ρ = 3.06 Mg·m−3

Crystallographic Data

Cell Parameters

Published Data
Standardized Data
Unit Cell
Niggli-Reduced Cell
Space Group
a
b
c
α
β
γ
a/b
b/c
c/a
V

Atom Coordinates

Standardized

Site
Element
Wyckoff Symbol
Symmetry
X
Y
Z
Occupation
Co-ord. No.
Atomic Env.

Published

Site
Element
Wyckoff Symbol
Symmetry
X
Y
Z
Occupation

Displacement Parameters

Isotropic

Site
Published
U [nm2]
Type
Computed
Beq [nm2]

Experimental Details

Reference

3D Interactive Structure

About this content

  • Database name

    PAULING FILE Multinaries Edition – 2012

  • Dataset ID

    sd_1922245

  • Copyright

    ©Springer & Material Phases Data System (MPDS), Switzerland & National Institute for Materials Science (NIMS), Japan, 2016

  • Chief Editor

    Pierre Villars, Material Phases Data System (MPDS), CH-6354 Vitznau, Switzerland

    villars.mpds@bluewin.ch

  • Credits

    SpringerMaterials Release 2016.

    Data generated pre-2002: © Springer & MPDS & NIMS; post-2001: © Springer & MPDS

    All Rights Reserved. Version 2016.10.

    Project Coordinator: Shuichi Iwata

    Section-Editor: Karin Cenzual (Crystal Structures)

  • Cite this content

    Citation copied